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Beilstein J. Org. Chem. 2014, 10, 794–807, doi:10.3762/bjoc.10.75
Graphical Abstract
Figure 1: Structure of the central cores and lengthening arms.
Scheme 1: Synthesis of compounds of series I–III.
Scheme 2: Synthesis of compounds of series IV–VI.
Figure 2: Chemical formulae of studied compounds I–VI.
Figure 3: DSC plots for compounds a) IIb, b) IVb and c) Vb taken on second heating (upper curve) and cooling ...
Figure 4: Planar texture of Ib in the SmCAPA phase at temperature T = 130 °C (a) without field, and (b) in th...
Figure 5: Planar texture of IIb (a) at the phase transition from the SmAP (upper right corner) to the SmCAPA ...
Figure 6: Switching current for compound IIb at T = 150 °C, taken in the SmCAPA phase at a triangular field, E...
Figure 7: Planar texture of IIb compound the SmCSPA phase at T = 130 °C, (a) without applied field and (b) in...
Figure 8: Temperature dependence of the layer spacing value, d, and intensity of the corresponding X-ray sign...
Figure 9: X-ray patterns of a partially aligned sample of IIb in (a) the SmCG phase at 148 °C and (b) in the ...
Figure 10: 3-Dimensional plot of the imaginary part of permittivity, ε’’, versus temperature and frequency for ...
Figure 11: Temperature dependence of the dielectric strength, Δε, and relaxation frequency, fr, for IIb.
Figure 12: Schematic organization of bent-shaped molecules in layers for the SmCAPA–SmCG–SmCSPA sequence of me...